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Salt-Mediated Coarsening in Conversion-Reaction-Synthesized Nanoporous Metals and Nanocomposites Resolved through In Situ Synchrotron Diffraction Studies

https://doi.org/10.1021/acs.chemmater.2c03786

Corrao, Adam A; Mattei, Gerard S; Coaty, Christopher M; Li, Zhuo; Petrova, Victoria; Yin, Liang; Liu, Ping; Khalifah, Peter G (July 2023, Chemistry of Materials)

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Thermodynamic and Kinetic Barriers Limiting Solid-State Reactions Resolved through In Situ Synchrotron Studies of Lithium Halide Salts

https://doi.org/10.1021/acs.chemmater.2c02543

Cosby, Monty R.; Bartel, Christopher J.; Corrao, Adam A.; Yakovenko, Andrey A.; Gallington, Leighanne C.; Ceder, Gerbrand; Khalifah, Peter G. (February 2023, Chemistry of Materials)

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Assessing Thermodynamic Selectivity of Solid-State Reactions for the Predictive Synthesis of Inorganic Materials

https://doi.org/10.1021/acscentsci.3c01051

McDermott, Matthew J; McBride, Brennan C; Regier, Corlyn E; Tran, Gia Thinh; Chen, Yu; Corrao, Adam A; Gallant, Max C; Kamm, Gabrielle E; Bartel, Christopher J; Chapman, Karena W; et al (October 2023, ACS Central Science)

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Morphological Control of Nanoporous Copper Formed from Conversion Reaction Synthesis

https://doi.org/10.1021/acs.jpcc.2c03544

Feng, Shijie; Petrova, Victoria; Corrao, Adam A.; Wang, Shen; Yang, Kesong; Khalifah, Peter G.; Liu, Ping (September 2022, The Journal of Physical Chemistry C)

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Synthesis of flexible Co nanowires from bulk precursors

https://doi.org/10.1039/d2ra03790d

Petrova, Victoria; Corrao, Adam A.; Wang, Shen; Xiao, Yuxuan; Chapman, Karena W.; Fullerton, Eric E.; Khalifah, Peter G.; Liu, Ping (July 2022, RSC Advances)

This work reports a method of producing flexible cobalt nanowires (NWs) directly from the chemical conversion of bulk precursors at room temperature. Chemical reduction of Li 6 CoCl 8 produces a nanocomposite of Co and LiCl, of which the salt is subsequently removed. The dilute concentration of Co in the precursor combined with the anisotropic crystal structure of the hcp phase leads to 1D growth in the absence of any templates or additives. The Co NWs are shown to have high saturation magnetization (130.6 emu g −1 ). Our understanding of the NW formation mechanism points to new directions of scalable nanostructure generation.
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